冀西北宣化盆地髫髻山组粗面岩年代学、地球化学特征及其地质意义

doi:10.11720/wtyht.2024.2503

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Abstract

The Tiaojishan Formation in northwestern Hebei Province is home to volcanic-sedimentary strata. Due to the lack of fossil organisms, insufficient isotopic dating data, and outdated dating methods, the formation epochs of these strata have been controversial. To accurately determine their formation epochs and examine their regional geotectonic setting, this study conducted a detailed field investigation of the lithologic assemblage of the Tiaojishan Formation in the Xuanhua Basin. Petrological, petrogeochemical, and high-precision isotopic dating studies were conducted on the trachytic volcanic rocks in the upper segment of the formation, obtaining the LA-ICP-MS-based zircon U-Pb isotopic ages, which were 161.1±1.2 Ma and 162.5±1.3Ma. As indicated by the petrological and petrogeochemical characteristics, these trachytic volcanic rocks belong to the shoshonite series, exhibiting enriched light rare earth elements, relatively enriched elements including Rb, K, Th, Ce, Zr, and Hf, and relatively depleted Ba, Nb, Sr, P, and Ti. According to the comparison of principal parameters and graphical discrimination, the magma originated primarily from the melting of continental crustal materials and formed in the tectonic setting of compressional continental margin volcanic arcs. The comprehensive research reveals that the Tiaojishan Formation formed primarily during the Middle Jurassic and continued to the Late Jurassic, and the trachytic volcanic rocks in its upper segment formed in the intraplate compressional tectonic setting. The results of this study provide new data for the division and correlation of Mesozoic volcanic-sedimentary strata and the analysis of their formation environment.

Key words： Xuanhua Basin Tiaojishan Formation trachyte petrogeochemical characteristics zircon U-Pb

Received: 08 October 2022 Published: 26 February 2024

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	Ji-Yuan YANG
	Xin-Zhuo HU
	Jing ZHOU
	Peng-Chao QI
	Ze-Yang LI
	Jia-Bao MENG
	Fan XU
	Hui-Bin ZHANG
	Hui-Yun QI

Cite this article:

Ji-Yuan YANG,Xin-Zhuo HU,Jing ZHOU, et al. Chronology and geochemical characteristics of trachytes in the Tiaojishan Formation, Xuanhua Basin, northwestern Hebei Province, and their geological implications[J]. Geophysical and Geochemical Exploration, 2024, 48(1): 1-14.

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https://www.wutanyuhuatan.com/EN/10.11720/wtyht.2024.2503 OR https://www.wutanyuhuatan.com/EN/Y2024/V48/I1/1

31])and geological sketch (b) of the Xuanhua Basin (simplified according to Bai C D,et al^[32])
1—Quaternary;2—Zhangjiakou Formation;3—Tuchengzi Formation;4—the second section of Tiaojishan Formation;5—the first section of Tiaojishan Formation;6—Jiulongshan Formation;7—Wumishan Formation;8—Gaoyuzhuang Formation;9—granite porphyry;10—angle unconformity contact boundary;11—normal fault and dip;12—fault of unknown nature;13—Feilaifeng structure;14—formation occurrrence;15—volcanic crater;16—sampling position
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Sketch map of the regional structure (a) (simplified according to Zhen S M, et al. ^[31])and geological sketch (b) of the Xuanhua Basin (simplified according to Bai C D,et al^[32])
1—Quaternary;2—Zhangjiakou Formation;3—Tuchengzi Formation;4—the second section of Tiaojishan Formation;5—the first section of Tiaojishan Formation;6—Jiulongshan Formation;7—Wumishan Formation;8—Gaoyuzhuang Formation;9—granite porphyry;10—angle unconformity contact boundary;11—normal fault and dip;12—fault of unknown nature;13—Feilaifeng structure;14—formation occurrrence;15—volcanic crater;16—sampling position

Field outcrops(a~d) and photomicrographs(e~f) of trachytes in the Tiaojishan Formation, Xuanhua Basin (Kfs: potassium feldspar)

样品号	含量/10^-6				同位素比值								年龄/Ma
样品号	Pb	²³²Th	²³⁸U	Th/U	²⁰⁷Pb/ ²³⁵U	2σ	²⁰⁶Pb/ ²³⁸U	2σ	²⁰⁷Pb/ ²⁰⁶Pb	2σ	²⁰⁸Pb/ ²³²Th	2σ	²⁰⁶Pb/ ²³⁸U	2σ	²⁰⁷Pb/ ²³⁵U	2σ	²⁰⁸Pb/ ²³²Th	2σ
D2022-1	3.0	62.5	94.0	0.66	0.177	0.021	0.0251	0.0007	0.0515	0.006	0.0081	0.0007	159.7	4.5	162.0	18.0	162.0	14.0
D2022-2	2.6	66.1	77.4	0.85	0.181	0.028	0.0253	0.0008	0.0530	0.009	0.0086	0.0007	161.0	5.3	162.0	24.0	174.0	14.0
D2022-3^*	6.0	57.2	82.9	0.69	1.490	0.190	0.0305	0.0014	0.3230	0.034	0.0399	0.0043	193.6	8.5	829.0	73.0	784.0	82.0
D2022-4	2.3	46.0	74.5	0.62	0.179	0.029	0.0254	0.0011	0.0504	0.008	0.0079	0.0010	161.9	6.8	160.0	25.0	160.0	21.0
D2022-5	3.2	63.3	100.8	0.63	0.164	0.021	0.0251	0.0007	0.0478	0.006	0.0086	0.0007	159.7	4.6	149.0	18.0	173.0	13.0
D2022-6	2.8	58.3	85.7	0.68	0.165	0.021	0.0253	0.0007	0.0485	0.006	0.0083	0.0007	161.3	4.7	149.0	19.0	167.0	13.0
D2022-7	2.8	58.7	84.6	0.69	0.178	0.024	0.0254	0.0008	0.0513	0.007	0.0085	0.0007	161.8	4.7	161.0	21.0	170.0	13.0
D2022-8	2.7	48.8	88.6	0.55	0.166	0.019	0.0251	0.0008	0.0477	0.006	0.0083	0.0009	159.7	4.7	151.0	17.0	166.0	18.0
D2022-9	2.1	36.3	67.6	0.54	0.162	0.025	0.0255	0.0008	0.0458	0.007	0.0093	0.0009	162.0	5.1	145.0	22.0	187.0	17.0
D2022-10	2.6	45.8	81.0	0.56	0.175	0.021	0.0253	0.0007	0.0531	0.007	0.0089	0.0008	161.0	4.4	158.0	18.0	180.0	15.0
D2022-11	2.9	57.3	82.9	0.69	0.201	0.037	0.0253	0.0009	0.0610	0.011	0.0093	0.0013	161.1	5.4	176.0	31.0	187.0	27.0
D2022-12	2.4	46.6	80.6	0.58	0.175	0.033	0.0251	0.0009	0.0498	0.009	0.0084	0.0010	160.0	5.7	157.0	28.0	169.0	20.0
D2022-13	2.4	39.9	73.2	0.55	0.163	0.035	0.0250	0.0010	0.0500	0.010	0.0097	0.0013	159.3	6.5	148.0	31.0	194.0	27.0
D2022-14	2.1	39.8	64.9	0.61	0.175	0.026	0.0251	0.0008	0.0500	0.008	0.0080	0.0008	159.7	4.9	154.0	22.0	162.0	17.0
D2022-15	1.6	30.2	53.4	0.57	0.169	0.040	0.0257	0.0012	0.0500	0.012	0.0080	0.0012	163.6	7.5	154.0	36.0	161.0	23.0
D2022-16	2.9	56.6	83.5	0.68	0.191	0.025	0.0256	0.0009	0.0552	0.007	0.0088	0.0009	163.0	5.8	174.0	22.0	177.0	18.0
D2022-17	3.3	88.8	92.9	0.96	0.201	0.046	0.0261	0.0014	0.0570	0.014	0.0084	0.0013	166.0	8.7	181.0	39.0	169.0	26.0
D2022-18	1.7	30.1	52.8	0.57	0.166	0.035	0.0254	0.0011	0.0480	0.010	0.0091	0.0013	161.3	6.9	148.0	30.0	182.0	26.0
D2022-19	1.9	32.8	59.8	0.55	0.180	0.032	0.0250	0.0010	0.0540	0.010	0.0084	0.0013	159.2	6.6	160.0	27.0	169.0	26.0
D2022-20	2.0	39.1	62.4	0.63	0.174	0.025	0.0257	0.0009	0.0502	0.008	0.0088	0.0010	163.7	5.6	158.0	22.0	176.0	20.0

Chronological analysis results of trachyte (D2022) zircon by LA-ICP-MS

样品号	含量/10^-6				同位素比值								年龄/Ma
样品号	Pb	²³²Th	²³⁸U	Th/U	²⁰⁷Pb/ ²³⁵U	2σ	²⁰⁶Pb/ ²³⁸U	2σ	²⁰⁷Pb/ ²⁰⁶Pb	2σ	²⁰⁸Pb/ ²³²Th	2σ	²⁰⁶Pb/ ²³⁸U	2σ	²⁰⁷Pb/ ²³⁵U	2σ	²⁰⁸Pb/ ²³²Th	2σ
D3511-1^*	7.7	151.8	187.0	0.81	0.24	0.035	0.0326	0.0008	0.05	0.0075	0.0112	0.0010	206.9	4.8	217.0	29.0	226.0	21.0
D3511-2	64.9	2168.0	1695.0	1.28	0.18	0.007	0.0256	0.0005	0.05	0.0016	0.0080	0.0002	162.8	2.8	167.0	5.7	161.3	3.4
D3511-3^*	29.8	509.0	455.0	1.12	0.33	0.016	0.0452	0.0008	0.05	0.0026	0.0142	0.0004	285.1	4.8	285.0	12.0	285.8	7.3
D3511-4^*	105.9	100.7	462.0	0.22	2.07	0.072	0.1869	0.0037	0.08	0.0028	0.0629	0.0033	1104.0	20.0	1136.0	24.0	1232.0	62.0
D3511-5^*	15.6	117.4	206.1	0.57	0.46	0.044	0.0593	0.0013	0.06	0.0055	0.0186	0.0013	371.5	7.9	378.0	31.0	372.0	25.0
D3511-6^*	19.1	331.2	498.0	0.67	0.21	0.017	0.0282	0.0008	0.05	0.0049	0.0087	0.0006	179.1	4.9	193.0	14.0	174.0	12.0
D3511-7^*	15.7	207.2	241.0	0.86	0.34	0.026	0.0459	0.0010	0.05	0.0041	0.0149	0.0007	289.2	6.1	292.0	20.0	299.0	14.0
D3511-8^*	13.2	250.8	190.6	1.32	0.35	0.033	0.0458	0.0013	0.06	0.0054	0.0138	0.0008	288.6	8.0	299.0	25.0	277.0	16.0
D3511-9^*	34.1	490.0	486.0	1.01	0.37	0.016	0.0494	0.0009	0.05	0.0024	0.0153	0.0004	311.0	5.2	315.0	12.0	307.3	7.7
D3511-10	22.4	600.0	647.0	0.93	0.18	0.007	0.0255	0.0004	0.05	0.0021	0.0083	0.0002	162.4	2.4	165.8	6.3	166.7	4.4
D3511-11	16.6	351.7	503.4	0.70	0.18	0.010	0.0255	0.0005	0.05	0.0029	0.0078	0.0003	162.2	2.9	166.7	8.9	157.5	6.5
D3511-12^*	29.2	502.0	441.0	1.14	0.35	0.033	0.0447	0.0013	0.06	0.0048	0.0141	0.0007	281.7	7.9	303.0	24.0	282.0	13.0
D3511-13	9.0	221.6	265.0	0.84	0.18	0.012	0.0257	0.0005	0.05	0.0032	0.0082	0.0003	163.5	3.1	164.0	10.0	165.5	6.4
D3511-14^*	198.1	109.7	304.0	0.36	11.80	0.190	0.4927	0.0073	0.17	0.0022	0.1374	0.0028	2581.0	32.0	2586.0	15.0	2601.0	50.0
D3511-15	3.5	90.1	96.1	0.94	0.19	0.027	0.0253	0.0008	0.05	0.0074	0.0086	0.0006	161.1	4.7	168.0	23.0	174.0	13.0
D3511-16^*	39.3	493.0	591.0	0.83	0.35	0.035	0.0473	0.0012	0.05	0.0056	0.0155	0.0008	297.6	7.2	303.0	26.0	310.0	16.0
D3511-17	45.6	699.0	596.0	1.17	0.65	0.028	0.0488	0.0009	0.10	0.0046	0.0192	0.0005	307.2	5.7	500.0	17.0	384.0	10.0
D3511-18^*	234.3	342.3	311.5	1.10	11.59	0.190	0.4840	0.0074	0.17	0.0028	0.1335	0.0022	2543.0	32.0	2573.0	15.0	2532.0	40.0

Chronological analysis results of trachyte (D3511) zircon by LA-ICP-MS

样品号	PM17-38-1	PM17-41-1	PM17-44-1	D2022	D3511	D4021-1	D4021-2	D4022-1
SiO₂	64.60	65.62	63.35	68.96	63.18	62.72	61.19	63.96
TiO₂	0.90	0.97	0.99	0.34	0.99	1.04	1.02	0.96
Al₂O₃	13.76	14.52	14.64	15.46	14.55	15.34	15.24	14.47
Fe₂O₃	5.83	4.42	6.66	1.43	5.40	6.50	8.63	7.72
FeO	0.33	0.55	1.14	0.49	0.63	0.18	0.18	0.12
MnO	0.137	0.076	0.12	0.040	0.130	0.042	0.066	0.043
MgO	0.45	0.50	0.55	0.87	1.34	0.39	0.51	0.32
CaO	2.26	1.55	0.90	2.35	1.57	1.07	1.20	1.11
Na₂O	4.00	4.37	4.39	3.45	4.31	4.18	3.79	3.20
K₂O	5.45	5.75	5.81	4.34	5.63	6.10	5.86	5.74
P₂O₅	0.282	0.312	0.32	0.149	0.330	0.337	0.324	0.306
灼失量	1.87	1.19	0.89	1.83	1.77	2.00	1.88	1.97
Total	99.91	99.89	99.88	99.76	99.90	99.89	99.89	99.91
A/NK	1.10	1.08	1.08	1.49	1.10	1.14	1.21	1.26
A/CNK	0.87	0.94	1.02	1.08	0.95	1.05	1.09	1.13
La	51.90	55.50	53.70	43.20	52.70	45.40	54.00	53.20
Ce	96.10	105.00	108.00	74.30	99.60	93.70	109.00	112.00
Pr	12.90	13.50	13.60	7.86	12.70	12.00	13.30	13.60
Nd	49.70	51.50	52.40	27.50	49.40	47.40	51.70	53.00
Sm	9.57	9.16	9.03	4.04	9.14	9.17	9.34	9.80
Eu	2.74	2.84	2.81	1.30	2.68	3.41	3.09	2.95
Gd	8.57	7.86	8.16	3.47	7.83	8.33	8.29	8.73
Tb	1.37	1.26	1.30	0.48	1.30	1.40	1.38	1.47
Dy	7.96	7.07	7.09	2.30	7.69	6.84	7.09	7.74
Ho	1.50	1.34	1.40	0.44	1.46	1.24	1.35	1.51
Er	4.05	3.65	4.07	1.39	4.15	3.43	3.87	4.34
Tm	0.60	0.54	0.68	0.22	0.65	0.49	0.58	0.68
Yb	3.66	3.17	4.18	1.60	3.98	2.85	3.57	4.20
Lu	0.57	0.48	0.63	0.26	0.64	0.42	0.53	0.61
Y	38.70	34.50	37.80	13.20	38.60	31.80	33.90	41.10
Rb	101.00	106.00	108.00	101.00	90.10	92.90	101.00	103.00
Ba	356.00	386.00	370.00	1255.00	340.00	377.00	312.00	267.00
Th	7.99	8.21	7.84	7.84	7.45	8.24	9.05	8.80
U	1.62	1.69	1.62	1.23	1.88	1.53	1.51	1.71
Nb	19.70	21.00	20.90	13.80	19.80	18.90	19.80	19.90
Sr	36.90	31.00	32.20	433.00	54.80	74.40	38.80	46.60
Zr	325.00	358.00	375.00	147.00	336.00	369.00	379.00	385.00
Hf	8.44	8.69	8.86	4.05	8.25	9.27	9.26	9.02
Ga	23.00	24.70	24.50	16.00	24.00	23.80	24.50	24.60
Ta	1.12	1.13	1.35	1.00	1.09	1.21	1.21	1.14
V	12.00	7.02	6.62	28.40	5.12	51.80	24.40	35.50
Co	2.11	1.09	1.25	3.26	2.38	1.84	1.29	0.91
Ni	3.33	1.97	2.87	2.46	3.02	1.13	0.98	1.26
∑REE	251.16	262.49	267.08	168.47	253.92	236.10	267.00	273.96
LREE	222.90	237.13	239.57	158.30	226.22	21110.00	240.34	244.68
HREE	28.27	25.36	27.52	10.16	27.69	25.00	26.65	29.29
LREE/ HREE	7.89	9.35	8.71	15.57	8.17	8.45	9.02	8.35
La/Yb	10.19	12.54	9.22	19.34	9.51	11.46	10.87	9.08
δEu	0.92	1.02	1.00	1.06	0.97	1.19	1.07	0.97
δCe	0.91	0.94	0.98	0.99	0.94	0.99	0.99	1.02

Analysis results of major elements (%), trace elements and rare earth elements (10^-6) of trachytes in the Tiaojishan Formation

Zircon cathodoluminescence images of trachytes in the Tiaojishan Formation, Xuanhua Basin

Consonance map and weighted average age of U-Pb ages of trachytes in the Tiaojishan Formation, Xuanhua Basin
a—D2022;b—D3511

39] and w(K₂O)-w(SiO₂) diagram (b)^[40-41]of trachytes in the Tiaojishan Formation, Xuanhua Basin
1—picrite basalt;2—basalt;3—basaltic andesite;4—andesite;5—dacite;6—rhyolite; 7—trachybasalt;8—basaltic trachyandesite;9—trachyandesite;10—trachyte,trachyte dacite; 11—phonolite;12—alkalinite phonolite;13—phonolitic alkali basalt;14—alkali basalt, basalt; 15—subfeldspar rock
">

TAS diagram (a) ^[39] and w(K₂O)-w(SiO₂) diagram (b)^[40-41]of trachytes in the Tiaojishan Formation, Xuanhua Basin
1—picrite basalt;2—basalt;3—basaltic andesite;4—andesite;5—dacite;6—rhyolite; 7—trachybasalt;8—basaltic trachyandesite;9—trachyandesite;10—trachyte,trachyte dacite; 11—phonolite;12—alkalinite phonolite;13—phonolitic alkali basalt;14—alkali basalt, basalt; 15—subfeldspar rock

42],primitive mantle normalized values according to Sun and McDonough^[43])
">

Chondrite-normalized rare earth element distribution map (a) and spider diagram of primitive mantle normalized trace elements (b) of trachytes in the Tiaojishan Formation, Xuanhua Basin(standardized values for chondrites according to Bounton^[42],primitive mantle normalized values according to Sun and McDonough^[43])

Harker diagram of major elements of trachytes in the Tiaojishan Formation, Xuanhua Basin

53] and Sr/Y—Y diagram (b)^[54] of trachytes in the Tiaojishan Formation,Xuanhua Basin
">

A/FM—C/FM diagram (a)^[53] and Sr/Y—Y diagram (b)^[54] of trachytes in the Tiaojishan Formation,Xuanhua Basin

64?-66]
WPG—intraplate granite; VAG—volcanic arc granite; syn-COLG—syncolliding granite; ORG—mid-ocean ridge plagiogranite;1—mantle plagioclase granite; 2 —destructive active plate margin (pre-plate collision) granite; 3—post-plate collision uplift granite; 4—late orogenic granite; 5—A-type granite in non-orogenic mountains; 6—syncollision S-type granite; 7—post-orogenic A-type granite
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Discrimination map of trachytes in the Tiaojishan Formation, Xuanhua Basin^[64?-66]
WPG—intraplate granite; VAG—volcanic arc granite; syn-COLG—syncolliding granite; ORG—mid-ocean ridge plagiogranite;1—mantle plagioclase granite; 2 —destructive active plate margin (pre-plate collision) granite; 3—post-plate collision uplift granite; 4—late orogenic granite; 5—A-type granite in non-orogenic mountains; 6—syncollision S-type granite; 7—post-orogenic A-type granite

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